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New Mexico State University
College of Arts and Sciences
Department of Chemistry and Biochemistry

 

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   Department of Chemistry and Biochemistry

   I N S T R U M E N T A L    W E B    S I T E    M A P

    Chemical  Instrumentation  Laboratories  

 Spectroscopy

     Nuclear Magnetic Resonance Spectroscopy (NMR)
                  Sample Preparation
                  NMR Safety
                  Selecting NMR Solvents
                  Protocol for Obtaining Proton Spectra with the Gemini Instruments
                       Caution:  NMR Turbine Sample Holder
           
Table -- Why NMR 'Run' Parameters are Selected
                  Beginner Procedure for Obtaining Proton Spectra with the Gemini Instruments
                  Conversion of Gemini Data withVHelper
                  Remote Processing of Gemini Data -- NMR SpecManager
                  External Links on Fundamentals:
                       
NMR Basics
                       
Shimming
                       Run an NMR On Line
                       Example FID's
                    NMR Probes
                    View Inside of a Super Magnet

                         Gemini 200 (Room 38)
                             Variable Temperature
                             Homonuclear Decoupling
                             Shimming Values

                        NMR System 300 (Room 130)
                             Shimming Values

                        Unity 400 (Room 130) 
                             General Procedures for Obtaining NMR Spectra with the Unity 400
                              Procedure for Printing NMR Spectra from the Unity 400
                                   Stepwise Procedure for Protons with the Unity 400
                                   Stepwise Procedure for Carbon with the Unity 400
                                        NMR Deuterated Solvents
                                   One Pulse and 2-D COSY Experiments
                                   VNRM Parameters and Consequences
                                   
Anazasi FT-NMR

                     Protocol for Spectrometer Reservations
                     Form for Submitting Liquid NMR Sample for Unity 400
                  NMR Standards
                  Magnet Records
               
Support Staff Procedures
                     Cryogenic Magnet Service Liquid Nitrogen and Helium
                     Specific Cryogenic Procedure for Liquid Helium
                     Magnet Liquid Helium Records for Volume and Depth
                     Storage Dewar Relationship between Volume and Depth 
                     Vacuum Service for the Gemini 200

            FTIR
               Infrared Tutorial
               FTIR Instruments
            UV/VIS
                 Colorimeters Spectronic 20
                 Klett-Summerson Colorimeter
                 Diode Array Spectrometer (HP 8452A)

                 Agilent 8453 UV/Visible Diode Array
                Cary UV/VIS Spectrophotometer

                Circular Dichroism -- JASCO 810 CD Spectropolarimeter

          Raman

                Delta Nu Advantage 200A
         Fluorescence

                Spectrophotofluorometer (Aminco-Bwman Spectrophotofluorometer, 768-H)
                Cary Eclipse Fluorescence Spectrophotometer

           Perkin-Elmer LS 55 Luminescence Spectrometer
        Flame and Graphite AAS

             AAnalysis 800 Atomic Absorption Spectrometer    
   S e p a r a t i o n s
          Gas Chromatography  and GC/MS
                 Instrumentation and Tutorial
          ICP/MS and ICP Perkin-Elmer 2100 DV
          Centrifuge
              Procedure Beckman L8-M
              Procedure Beckman L5-65
           MS/HPLC
               Detailed Procedure Obtaining Mass Spectra with the Extrel Benchmark
                Agilent 1200 HPLC
    R e s o u r c e s
        Emergency Procedures
                Procedure for Restarting Instruments after a Power Failure
                Alarm Reset Procedure
                General Emergency Alarm Procedures
          Electronic Fabrication and Repair
          General Repair Vacuum Pumps, etc.
          Lypohilization and Vacuum Oven Drying
          Ultrasonic Cleaning
          High Purity Water
          Keyless Security Locks
          Muffle Furnace
          Location Classroom, Laboratories, and Offices
               Building 55
               Building 65
               Building 95
        Location of Departmental Property
      Forms for Laboratory Services or Repair
               Work Order for for Repair of Electronic Equipment,Vacuum Pumps, etc.
               Form for Liquid NMR Samples for the Unity 400
               Form for Mass Spectrum Analysis for Molecular Weight with the Extrel Quadropole
T e a c h i n g   L a b o r a t o r y   I n s t r u m e n t s
    Atomic Spectroscopy
        Chem 2000 Visible (Diode Array)
        Atomic Absorption (AAS)
        Direct Current Plasma (DCP)
        Anazasi FT-NMR
        Inductively Coupled Plasma (ICP)
   Separations
         Ion Chromatography (IC)
         Liquid Chromatography (LC and HPLC)
         ICP/Mass Spectroscopy (MS)
         Capillary Electrochromatography (CEC)
         Electrochemical Voltametry (CV)
         Ion Selective Electrodes (ISE)

 L i n k s   a n d   A c k n o w l e d g m e n t s
       Standard Reference Materials
        Site Map (this page)
       Staff for Instrumental and Electronic Shop
            List of Technical Publication
       Emergency Procedures
          Procedure for Restarting Instruments after a Power Failure
          Alarm Reset Procedure
          General Emergency Alarm Procedures

Return to Instrumentation or Teaching Instruments