College of Arts and Sciences
Department of Chemistry and Biochemistry
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Proton, 13Carbon, Phosphorus, Flurine, etc. Variable Temperature, DEPT, COSY, HMQC, and solvent suppressionHigh Sensitivity Probe |
Proton and 13C Spectra; Homonuclear decoupling, Varible TemperatureHigh Sensitivity Probe |
Proton, 13 Carbon, Phosphorus, etc. spectra with 5 and 10 mm, Inverse proton, and solids probes. HomoNuclear Decoupling, Variable Temperature |
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Queue System Maximum Time: 15 minutes |
0700-2000 Maximum of 30 minute blocks with two consecutive blocks allowed for an hour 2000-0700* Time blocks of any length can be reserved. |
Blocks of any time length can be reserved. | Always Reserved for Special Applications. Request permission. Also reserved for class instruction during Spring semester. |
0700-2000 Queue system blocks of 30 minutes can be reserved 2000-0700 Any time length blocks. |
*If you are using an instrument overnight you must come in before 8 AM to stop overnight experiments OR:
a. Leave instructions for the next user to print the spectra.
b. There is also a possibility of saving the last experiment to floppy. Blank formatted floppies and instructions are on the console. These floppies will only work on the Gemini instruments. Use DG to find the user and save to that name, e.g. SVF(DSK5.name). The user's data is returned by RT(DSK5.name) or processed through VHelper and SpecManager.
c. Overnight experiments could be conducted by selecting JEXP3, 4, 5, or 6. Leave a note for the morning user to change the experiment number.
d. All users must use the physical record their name, date, etc. in the log book for each instrument..